The insitu monitoring of MOFs by ball milling is an indispensable requirement for the indepth study of the ball milling reaction [35,51,53,60,71,106]. Although many kinds of MOFs have been successfully synthesized by ball milling, the understanding of the reaction mechanism of these MOFs is still insufficient.
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WhatsApp: +86 18203695377Ball milling experiments were done in a high energy planetary ball mill at a rotating speed of 300 rpm. To avoid the occurrence of any undesirable polluted phases, the ballmilling experiments were halted periodically (every ks) and then restarted when the temperature of the vial reached about 300 K.
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WhatsApp: +86 18203695377A comparative study was carried out for an alloy of Al 50 (Ni 75 Mo 25) 50 processed by two different high energy ball mills. A SPEX and Simoloyer mill were used.
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